From: Russell Vernon <russellnvernon**At_Symbol_Here**gmail.com>
Subject: Re: [DCHAS-L] C&EN: Setup may make transferring tert -butyl lithium and other pyrophoric reagents safer
Date: Mon, 18 Jun 2018 16:02:06 -0700
Reply-To: ACS Division of Chemical Health and Safety <DCHAS-L**At_Symbol_Here**PRINCETON.EDU>
Message-ID: CAEv1zv29B9FZ3ueD9U+q=kOKmU=Vton6nxLnQW9q4QZzcwy4Pg**At_Symbol_Here**mail.gmail.com
In-Reply-To


Seems to make it a closed system transfer, pretty clever

On Mon, Jun 18, 2018 at 11:34 AM DCHAS Membership Chair <membership**At_Symbol_Here**dchas.org> wrote:
Note a cameo role by a DCHAS regular in this article...

- Ralph

Setup may make transferring tert -butyl lithium and other pyrophoric reagents safer

Simple pieces of equipment decrease the danger of moving small volumes of chemicals prone to igniting

When chemists want to transfer a small amount of a pyrophoric reagent, such as tert-butyl lithium, they typically use a needle and syringe. But this protocol can be dangerous: One wrong move and the chemical could drip, or worse, squirt out of the needle and ignite. Chemists at Aarhus University have devised a simple setup and protocol that can make such transfers safer.
....
more at
https://cen.acs.org/safety/lab-safety/Setup-make-transferring-tert-butyl/96/web/2018/06

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